Bromomethyl 4-methoxyphenyl ketone → HCID 15388729, 화합물
반응식
[N:1]1[CH:6]=[CH:5][C:4]([C:7]2[S:8][CH2:9][C:10](=[O:13])[NH:11][N:12]=2)=[CH:3][CH:2]=1.[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([C:22]([CH2:24][Br:25])=[O:23])=[CH:18][CH:17]=1>C(O)C>[Br-:25].[CH3:14][O:15][C:16]1[CH:21]=[CH:20][C:19]([C:22]([CH2:24][N+:1]2[CH:2]=[CH:3][C:4]([C:7]3[S:8][CH2:9][C:10](=[O:13])[NH:11][N:12]=3)=[CH:5][CH:6]=2)=[O:23])=[CH:18][CH:17]=1참가 물질
4
실험 절차
2-(4-Pyridyl)-4H,6H-1,3,4-thiadiazin-5-one (1.88 g, 9.74 mmol) and 4'-methoxyphenacyl bromide (2.23 g, 9.74 mmol) were dissolved in absolute ethanol (40 ml) and stirred at room temperature for one day. The resultingprecipitate was collected by filtration and washed with absolute ethanol toobtain the titled compound (3.84g) as yellow powder.