1-Nitroanthraquinone → 1-(Butylamino)anthraquinone

HRID 1758079

반응식

HRID 1758079 반응식
[N+:1]([C:4]1[C:17]2[C:16](=[O:18])[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9](=[O:19])[C:8]=2[CH:7]=[CH:6][CH:5]=1)([O-])=O.[CH2:20](N)[CH2:21][CH2:22][CH3:23]>CN(C=O)C>[CH2:20]([NH:1][C:4]1[C:17]2[C:16](=[O:18])[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=3)[C:9](=[O:19])[C:8]=2[CH:7]=[CH:6][CH:5]=1)[CH2:21][CH2:22][CH3:23]

참가 물질

4

반응물 2

HCID 67041-NitroanthraquinoneHCID 8007Butylamine

생성물 1

HCID 672121-(Butylamino)anthraquinone

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

1-Nitroanthraquinone was reacted in DMF at 20° C. with 5 moles n-butylamine for 5 hours. The reaction produced 1-butylamino anthraquinone which was a deep red solid having a melting point of 78° to 79° C.

출처 및 근거

ORD 기록
ord-0b1c3e72bd4e48429e31aef4506224ea
출처 데이터셋
uspto-grants-1983_02
특허 번호
US04371694

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