Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1758199생성일: 2026년 10월 27일
2,2'-((1-Methylethylidene)bis(cyclohexane-4,1-diyloxymethylene))bisoxirane → 2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]cyclohexyl}propane
https://huagongshe.com/reaction/1758199
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,2'-((1-Methylethylidene)bis(cyclohexane-4,1-diyloxymethylene))bisoxirane | HCID 114514 | — |
| 반응물 | 7,7,9,9-Tetramethyl-1,4-dioxa-8-azaspiro[4.5]decane | HCID 567045 | — |
| 생성물 | 2,2-Bis{4-[2-hydroxy-3-(7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]dec-8-yl)propoxy]cyclohexyl}propane | HCID 20510600 | — |
반응 단계
A mixture of 8.8 g of 7,7,9,9-tetramethyl-1,4-dioxa-8-azaspiro[4.5]decane and 7.0 g of 2,2-bis[4-(2,3-epoxypropoxy)cyclohexyl]propane was heated at 120° C. for 30 hours. After completion of the reaction, the reaction mixture was purified by column chromatography through silica gel eluted with ethyl acetate. The desired Compound No. 207 was obtained in the form of a pale yellow oil which after being kept at ambient temperature, turned to a solid melting at 48°-50° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04371644 |
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| 출처 데이터셋 | uspto-grants-1983_02 |
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| ORD ID | ord-fa8fa4af90de4374802425b3daabc20e |
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| 출처 메모 | uspto-grants-1983_02 |
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