Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1758776생성일: 2026년 10월 27일
Cyclohexyl methacrylate → divinylbenzene cyclohexyl methacrylate N,N-diethylaminoethyl methacrylate
https://huagongshe.com/reaction/1758776
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Cyclohexyl methacrylate | HCID 7561 | — |
| 반응물 | Stearyltrimethylammonium chloride | HCID 8155 | — |
| 반응물 | Potassium Persulfate | HCID 24412 | — |
| 반응물 | 1,2-Diethenylbenzene | HCID 66666 | — |
| 반응물 | Sodium Bisulfite | HCID 23665763 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | divinylbenzene cyclohexyl methacrylate N,N-diethylaminoethyl methacrylate | HCID 70529907 | — |
반응 단계
216 g of distilled water was placed in a reaction vessel, deaerated with a nitrogen gas, and heated to 60° C. in the presence of the nitrogen gas. 15.8 g of stearyltrimethylammonium chloride, 0.07 g of polyvinyl alcohol, 33.7 g of cyclohexyl methacrylate, 37.1 g of N,N-diethylaminoethyl thacrylate, and 2.0 g of divinylbenzene were added thereto. Then, 0.44 g of potassium persulfate dissolved in 9.3 ml of distilled water deaerated with a nitrogen gas, and 0.14 g of sodium hydrogensulfite dissolved in 1.5 ml of distilled water deaerated with a nitrogen gas were simultaneously added thereto, and heated for about one hour. Subsequently, the above-described potassium persulfate aqueous solution and the sodium hydrogensulfite aqueous solution were again added thereto, followed by continuing heating for about 5 hours. Then, the system was cooled to room temperature, and filtered to obtain a polymer dispersion containing 22.8 wt% solids.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04374924 |
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| 출처 데이터셋 | uspto-grants-1983_02 |
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| ORD ID | ord-9ca22283ed3a4bdb91f2b44e8c000613 |
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| 출처 메모 | uspto-grants-1983_02 |
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