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HRID 1758776생성일: 2026년 10월 27일

Cyclohexyl methacrylate → divinylbenzene cyclohexyl methacrylate N,N-diethylaminoethyl methacrylate

https://huagongshe.com/reaction/1758776

반응식

참여 물질

역할이름HCID투입량
반응물Cyclohexyl methacrylateHCID 7561—
반응물Stearyltrimethylammonium chlorideHCID 8155—
반응물Potassium PersulfateHCID 24412—
반응물1,2-DiethenylbenzeneHCID 66666—
반응물Sodium BisulfiteHCID 23665763—
용매WaterHCID 962—
생성물divinylbenzene cyclohexyl methacrylate N,N-diethylaminoethyl methacrylateHCID 70529907—

반응 조건

온도60 °C

반응 단계

216 g of distilled water was placed in a reaction vessel, deaerated with a nitrogen gas, and heated to 60° C. in the presence of the nitrogen gas. 15.8 g of stearyltrimethylammonium chloride, 0.07 g of polyvinyl alcohol, 33.7 g of cyclohexyl methacrylate, 37.1 g of N,N-diethylaminoethyl thacrylate, and 2.0 g of divinylbenzene were added thereto. Then, 0.44 g of potassium persulfate dissolved in 9.3 ml of distilled water deaerated with a nitrogen gas, and 0.14 g of sodium hydrogensulfite dissolved in 1.5 ml of distilled water deaerated with a nitrogen gas were simultaneously added thereto, and heated for about one hour. Subsequently, the above-described potassium persulfate aqueous solution and the sodium hydrogensulfite aqueous solution were again added thereto, followed by continuing heating for about 5 hours. Then, the system was cooled to room temperature, and filtered to obtain a polymer dispersion containing 22.8 wt% solids.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04374924
출처 데이터셋uspto-grants-1983_02
ORD IDord-9ca22283ed3a4bdb91f2b44e8c000613
출처 메모uspto-grants-1983_02