Sodium Iodide → Monosodium monoethyl acetylphosphonate

HRID 1759159

반응식

HRID 1759159 반응식
[C:1]([P:4](=[O:11])([O:8]CC)[O:5][CH2:6][CH3:7])(=[O:3])[CH3:2].[I-].[Na+:13]>CC(CC)=O>[C:1]([P:4](=[O:8])([O-:11])[O:5][CH2:6][CH3:7])(=[O:3])[CH3:2].[Na+:13]

참가 물질

4

반응물 2

HCID 5238Sodium IodideHCID 522997Diethyl acetylphosphonate

생성물 1

HCID 23701875Monosodium monoethyl acetylphosphonate

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

A solution of diethyl acetylphosphonate (5 g, 0.028 mol) and oven-dried sodium iodide (4.2 g, 0.028 mol) in molecular sieve dried ethyl methyl ketone (75 ml) was stirred and refluxed for 16 hours.

후처리

  1. temperaturerefluxed for 16 hours

출처 및 근거

ORD 기록
ord-983cb2f816e6413e874478117333893a
출처 데이터셋
uspto-grants-1982_07
특허 번호
US04339443

연결된 노트

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