Sodium Iodide → HCID 23701878, 화합물

HRID 1759161노트

반응식

HRID 1759161 반응식
[C:1]([P:4]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:7])[O:5]C)(=[O:3])[CH3:2].[I-].[Na+:15]>CC(CC)=O>[C:1]([P:4]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)(=[O:5])[O-:7])(=[O:3])[CH3:2].[Na+:15]

참가 물질

4

반응물 2

HCID 5238Sodium IodideHCID 23264536Methyl acetyl(phenyl)phosphinate

생성물 1

HCID 23701878HCID 23701878, 화합물

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

Methyl acetylphenylphosphinate (5.0 g, 0.025 mol) was added to a solution of sodium iodide (3.8 g, 0.025 mol) in molecular sieve dried ethyl methyl ketone (50 ml) and the resulting solution was stirred and refluxed for 15 minutes.

후처리

  1. temperaturerefluxed for 15 minutes

출처 및 근거

ORD 기록
ord-cb111c3406314b5db8ba23a79db817c8
출처 데이터셋
uspto-grants-1982_07
특허 번호
US04339443

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