1-Nitro-4-tert-butyl-2,6-dimethylbenzene → 4-Tert-butyl-2,6-dimethylaniline

반응식

[N+:1]([C:4]1[C:9]([CH3:10])=[CH:8][C:7]([C:11]([CH3:14])([CH3:13])[CH3:12])=[CH:6][C:5]=1[CH3:15])([O-])=O.[H][H]>>[CH3:15][C:5]1[CH:6]=[C:7]([C:11]([CH3:13])([CH3:12])[CH3:14])[CH:8]=[C:9]([CH3:10])[C:4]=1[NH2:1]

참가 물질

반응물 2

HCID 2233901-Nitro-4-tert-butyl-2,6-dimethylbenzene

HCID 178418361HCID 178418361, 화합물

생성물 1

HCID 12296974-Tert-butyl-2,6-dimethylaniline

실험 절차

contacting the 2-nitro-1,3-dimethyl-5-tertiarybutylbenzene with hydrogen in the presence of a hydrogenation catalyst at a temperature of from about 0° C. to about 200° C. and a pressure of from about 0 psig to about 2000 psig to form 2,6-dimethyl-4-tertiary-butylaniline;

후처리

customof from about 0° C. to about 200° C.

출처 및 근거

ORD 기록: ord-9c897d71ff1b4763bdaac51772a0bea9
출처 데이터셋: uspto-grants-1982_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04340758

반응 노트

불러오는 중…