Sulfamide → HCID 178479209, 화합물

HRID 1762977

반응식

HRID 1762977 반응식
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].Cl.[Cl:7][CH2:8][CH2:9][C:10]#[N:11]>C(OCC)C>[ClH:7].[S:1]([NH:5][C:10](=[NH:11])[CH2:9][CH2:8][Cl:7])(=[O:3])(=[O:2])[NH2:4]

참가 물질

4

반응물 2

HCID 82267SulfamideHCID 867420433-Chloropropionitrile hydrogen chloride

생성물 1

HCID 178479209HCID 178479209, 화합물

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

후처리

  1. additionTo a stirred suspension of 9.61 g
  2. filtrationthe product is filtered off
  3. washwashed twice with acetone
  4. customdried

출처 및 근거

ORD 기록
ord-6ec711e95d084ee185c242200ab7ae81
출처 데이터셋
uspto-grants-1989_05
특허 번호
US04835281

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