Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → N-methyl-N-tert.-octylthiomethylamine hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1,3,5-Trimethyl-1,3,5-triazacyclohexane | HCID 7952 | — |
| 반응물 | Tert.-octylthiomethylamine | HCID 86735983 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | N-methyl-N-tert.-octylthiomethylamine hydrochloride | HCID 85866484 | — |
반응 단계
300 ml. of acetonitrile, 12.9 g. (0.1 mole) of 1,3,5-trimethylhexahydro-s-triazine; 43.8 g. (0.3 mole) of tert.-octylthiomethylamine and 12 g. of hydrogen chloride gas are reacted together in the manner of Example I. A yield of 43.7 g. (64.6% of theory) of the title compound is obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04111682 |
| 출처 데이터셋 | uspto-grants-1978_09 |
| ORD ID | ord-dba2278fae3647809136087c4a36efe9 |
| 출처 메모 | uspto-grants-1978_09 |