Potassium Iodide → Iodide Ion

HRID 1763891

반응식

HRID 1763891 반응식
[CH3:1][C:2]([CH2:5][C:6]([C:9]1[CH:14]=[CH:13][C:12]([O:15][CH2:16][CH2:17][O:18][CH2:19][CH2:20][OH:21])=[CH:11][CH:10]=1)([CH3:8])[CH3:7])([CH3:4])[CH3:3].[I-:22].[K+].[I:24]([O-])(=O)=O>O>[CH3:4][C:2]([CH2:5][C:6]([C:9]1[CH:10]=[CH:11][C:12]([O:15][CH2:16][CH2:17][O:18][CH2:19][CH2:20][OH:21])=[CH:13][CH:14]=1)([CH3:7])[CH3:8])([CH3:1])[CH3:3].[I:22][I:24].[I-:24]

참가 물질

6

반응물 3

HCID 4875Potassium IodideHCID 24775Poly(oxy-1,2-ethanediyl), alpha-((1,1,3,3-tetramethylbutyl)phenyl)-omega-hydroxy-, potassium salt (1:1)HCID 84927Iodate

생성물 2

HCID 30165Iodide IonHCID 131711250Molecular iodine;2-[2-[4-(2,4,4-trimethylpentan-2-yl)phenoxy]ethoxy]ethanol

시약·촉매·용매 1

HCID 962Water용매

실험 절차

In a suitable glass container is placed 9.9 gm. of octylphenoxypoly(ethyleneoxy) ethanol, dissolved in 50 ml. of water to which is added 0.1 gm. of potassium iodide. The mixture is then acid to a pH of below 3 and 0.02 gm. of iodate ion added with stirring. After standing for twenty-four hours, the solvent is evaporated under vacuum and the formed octylphenoxypoly-(ethyleneoxy)ethanol-iodine is obtained in substantially pure form, without iodide ions.

후처리

  1. waitAfter standing for twenty-four hours
  2. customthe solvent is evaporated under vacuum

출처 및 근거

ORD 기록
ord-ae98b13a9023434daef4b43ede3fff5e
출처 데이터셋
uspto-grants-1978_09
특허 번호
US04113857

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