Dimethyl Sulfide → (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide

HRID 1764

반응식

HRID 1764 반응식
[Br:1][CH2:2][C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH3:8][S:9][CH3:10]>CC(C)=O>[Br-:1].[C:3]([CH2:2][S+:9]([CH3:10])[CH3:8])([O:5][CH2:6][CH3:7])=[O:4]

참가 물질

4

반응물 2

HCID 1068Dimethyl SulfideHCID 7748Ethyl bromoacetate

생성물 1

HCID 78861(2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A solution of ethyl bromoacetate (265 g) and dimethyl sulfide (114 g) in acetone (500 mL) was stirred at room temperature. After three days, the title compound was isolated by filtration of the reaction mixture. Melting point 88°-90° C.

출처 및 근거

ORD 기록
ord-d735999e237040e79efd9e34aa9e36bf
출처 데이터셋
uspto-grants-1998_03
특허 번호
US05726320

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