Sulfuric Acid → 2-Benzyltoluene
반응식
[C:1]1(Cl)[CH:6]=[CH:5][CH:4]=[C:3]([CH3:7])[C:2]=1[CH3:8].O.O.B(F)(F)F.S(=O)(=O)(O)O>C1C=CC=CC=1>[CH2:7]([C:3]1[CH:4]=[CH:5][CH:6]=[CH:1][C:2]=1[CH3:8])[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1참가 물질
5
실험 절차
A solution of 70 parts of xylyl chloride in 240 parts of benzene is added to a mixture of 60 parts of boron fluoride dihydrate and 250 parts of 75 per cent strength by weight sulfuric acid at from 75° to 78° C, whilst stirring vigorously. After 6 hours, the organic phase is separated off and 82 parts (91.1% of theory) of o-benzyl-toluene boiling at 98° C at 0.2 mm Hg are isolated by distillation.
후처리
- customthe organic phase is separated off
출처 및 근거
- ORD 기록
- ord-6f1c2bee9b2e4207b184765b2719bca8
- 출처 데이터셋
- uspto-grants-1978_09
- 특허 번호
- US04117019
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