4-Hydrazinylbenzenesulfonamide hydrochloride → HCID 9864112, 화합물

HRID 1764789노트

반응식

HRID 1764789 반응식
[F:1][C:2]([F:14])([F:13])[C:3](=O)/[CH:4]=[CH:5]/[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.Cl.[S:16]([C:20]1[CH:25]=[CH:24][C:23]([NH:26][NH2:27])=[CH:22][CH:21]=1)(=[O:19])(=[O:18])[NH2:17]>>[S:16]([C:20]1[CH:21]=[CH:22][C:23]([N:26]2[CH:5]([C:6]3[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=3)[CH2:4][C:3]([C:2]([F:14])([F:13])[F:1])=[N:27]2)=[CH:24][CH:25]=1)(=[O:19])(=[O:18])[NH2:17]

참가 물질

3

반응물 2

HCID 27945674-Hydrazinylbenzenesulfonamide hydrochlorideHCID 60060523-Buten-2-one,1,1,1-trifluoro-4-phenyl-

생성물 1

HCID 9864112HCID 9864112, 화합물수율 73%

실험 절차

A solution of trans-1,1,1-trifluoro-4-phenyl-3-buten-2-one (5 mmol) and 4-sulfamylphenyl hydrazine hydrochloride (6 mmol) was subjected to Procedure 3. The title compound was obtained in 73% yield, m.p. 178-180° C.; C, H analysis (C18H15SO2N4F3.H2O):

출처 및 근거

ORD 기록
ord-684a1471cb6349b7982e2f11a193ac2d
출처 데이터셋
uspto-grants-2007_06
특허 번호
USRE039681E1

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