Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxyquinoline → 3-(Hydroxymethylidene)-1-phenylquinoline-2,4(1H,3H)-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxyquinoline | HCID 6038 | — |
| 반응물 | 4-Hydroxy-1-phenyl-1,2-dihydroquinolin-2-one | HCID 54676161 | — |
| 생성물 | 3-(Hydroxymethylidene)-1-phenylquinoline-2,4(1H,3H)-dione | HCID 135454227 | — |
반응 단계
Following the procedure set forth in Preparation B, 1- phenyl-4-hydroxy-2(1H)-quinolinone was converted to 1 -phenyl-3-formyl-4-hydroxy-(2(1H)-quinolinone. That the expected product was obtained was confirmed by the spectral data: MS: m/e 265 (M·+); NMR (DMSO): δ10.08 (s, 1H, CHO) ppm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05378694 |
| 출처 데이터셋 | uspto-grants-1995_01 |
| ORD ID | ord-65a4b71350594840aa49ee2192ba0d7d |
| 출처 메모 | uspto-grants-1995_01 |