Methyl 3-[(2-thienylmethyl)thio]propanoate → 3-[(2-Thienylmethyl)thio]propanoic acid, hydrazide

HRID 1768793노트

반응식

HRID 1768793 반응식
O1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][S:7][CH2:8][CH2:9][C:10]([NH:12][NH2:13])=[O:11].[S:14]1C=CC=C1CSCCC(OC)=O>>[S:14]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][S:7][CH2:8][CH2:9][C:10]([NH:12][NH2:13])=[O:11]

참가 물질

3

반응물 2

HCID 15225387Methyl 3-[(2-thienylmethyl)thio]propanoateHCID 635800953-[(2-Furanylmethyl)thio]propanoic acid, hydrazide

생성물 1

HCID 677803753-[(2-Thienylmethyl)thio]propanoic acid, hydrazide

실험 절차

3-[(2-thienylmethyl)thio]propanoic acid, hydrazide (56) was prepared in the manner that 3-[(2-furanylmethyl)thio]propanoic acid, hydrazide (12) was prepared (Example 12) on a 23 mmol scale from methyl 3-[(2-thienylmethyl)thio]propanoate (55). After the solvent was removed under vacuum, 2.77 g (69%) of the product, which was a water white viscous liquid, was recovered and was used immediately in the manner described in Example 57, below.

후처리

  1. customAfter the solvent was removed under vacuum, 2.77 g (69%) of the product, which
  2. customwas recovered

출처 및 근거

ORD 기록
ord-e8927149a6c34ca0b0afcdcf348def52
출처 데이터셋
uspto-grants-1995_01
특허 번호
US05378840

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