참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitrobenzene | HCID 7416 | — |
| 반응물 | Tetramethylammonium hydroxide dihydrate | HCID 22116808 | — |
| 용매 | Benzonitrile | HCID 7505 | — |
| 생성물 | Azoxybenzene | HCID 10316 | 45% |
반응 단계
A solution containing 10 g of nitrobenzene, 1.27 g of tetramethylammonium hydroxide dihydrate and 1 g of benzonitrile was stirred at 60° C. with nitrogen bubbled into the solution via a syringe needle for 1 hour. Analysis of a sample of the reaction product by HPLC revealed N-(4-nitrophenyl)-benzamide was produced in 45% yield and azoxybenzene was generated in 22% yield based on tetramethylammonium hydroxide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05380946 |
|---|
| 출처 데이터셋 | uspto-grants-1995_01 |
|---|
| ORD ID | ord-a3dae9cde94f4c1a9997e15f107d85fd |
|---|
| 출처 메모 | uspto-grants-1995_01 |
|---|
