Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Benzeneazodiphenylamine → Aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Benzeneazodiphenylamine | HCID 7575 | — |
| 반응물 | Cyclohexanol | HCID 7966 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 생성물 | Aniline | HCID 6115 | — |
| 생성물 | N-Phenyl-p-phenylenediamine | HCID 7564 | — |
반응 단계
A solution of 4-(phenylazo)diphenylamine (0.273 g), cyclohexanol (5 g) and potassium t-butoxide (1 g) was heated at reflux under nitrogen for 4 hours. Analysis of the reaction mixture by HPLC indicated all of the 4-(phenyazo)-diphenylamine was consumed. 4-aminodiphenylamine and aniline were produced in 99% yield based on 4-(phenylazo)diphenylamine charged.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05382691 |
| 출처 데이터셋 | uspto-grants-1995_01 |
| ORD ID | ord-c8e6b65f71374bab982a36394e8cf5ba |
| 출처 메모 | uspto-grants-1995_01 |