Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → HCID 178447917, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 3-Isopropylidenecyclobutanecarboxylate | HCID 20096179 | — |
| 반응물 | HCID 178447901 | HCID 178447901 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178447917 | HCID 178447917 | — |
반응 단계
A mixture of 0.11 mol of DCC add 50 ml of dichloromethane is added at 0° C. to a mixture of 0.1 mol of 3-isopropylidenecyclobutanecarboxylate [sic] (prepared by the method of Gripps et al., Am. Soc. 81 (1959), 2723-2728) 0.1 mol of 4-(trans-4-propylcyclohexyl)phenol and 100 ml of dichloromethane. After the mixture has been stirred at room temperature for 16 hours and the solid constituents have been removed, conventional work-up gives the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05384072 |
| 출처 데이터셋 | uspto-grants-1995_01 |
| ORD ID | ord-f3dec78be4c34ba098fbc50fb0163095 |
| 출처 메모 | uspto-grants-1995_01 |