Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexane → 4-(3-t-Butylureidomethyl)-1-aminomethylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | tert-Butyl isocyanate | HCID 62412 | — |
| 반응물 | 1,4-Benzenedimethanamine | HCID 68315 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-(3-t-Butylureidomethyl)-1-aminomethylbenzene | HCID 20096740 | 42.6% |
반응 단계
To a solution of 2.7 g p-xylylenediamine in 100 ml methylene dichloride, was added slowly with stirring 10 ml of a n-hexan solution containing 990 mg t-butyl isocyanate under ice cooling. Stirring was continued at room temperature for two hours, the solvent was distilled off under reduced pressure, and the residue was purified by silica gel column chromatography, giving 1 g of 4-(3-t-butylureidomethyl)-1-aminomethylbenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05384425 |
| 출처 데이터셋 | uspto-grants-1995_01 |
| ORD ID | ord-4e207b34aa9841a3af25a5dca6a8b1b0 |
| 출처 메모 | uspto-grants-1995_01 |