Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Alcohol → Benzyl 8-bromooctanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Alcohol | HCID 244 | — |
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 8-Bromooctanoic acid | HCID 548275 | — |
| 촉매 | 4-Pyrrolidinopyridine | HCID 75567 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Benzyl 8-bromooctanoate | HCID 11278409 | 100.2% |
반응 단계
This compound was prepared from 8-bromooctanoic acid (2.23 g; 10.0 mmol), benzyl alcohol (1.19 g; 11.0 mmol), N,N′-dicyclohexylcarbodiimide (DCC, 2.27 g; 11.0 mmol), and 4-pyrrolidinylpyridine (50 mg) in dry dichloromethane (50 mL) using Procedure A. 3.14 g (100%) product was obtained (clear oil that eventually solidified on standing).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09249086B2 |
| 출처 데이터셋 | uspto-grants-2016_02 |
| ORD ID | ord-1387cc3a850741b1bace81194970ff9f |
| 출처 메모 | uspto-grants-2016_02 |