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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 17720생성일: 2026년 10월 26일

4-(Dibenzofuran-2-yloxy)-1-nitrobenzene → 4-(Dibenzofuran-2-yloxy)aniline

https://huagongshe.com/reaction/17720

반응식

참여 물질

역할이름HCID투입량
반응물4-(Dibenzofuran-2-yloxy)-1-nitrobenzeneHCID 2102893—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물4-(Dibenzofuran-2-yloxy)anilineHCID 66977456—

반응 단계

The nitro intermediate (10 mmol) obtained above was dissolved in EtOAc (50 mL) and hydrogenated in the presence of 10% Pd/C (360 mg) until completion according to General Procedure H, as indicated by TLC or HPLC. The reaction mixture was then filtered to remove the catalyst. The solvent was removed in vacuuo to afford the desired 4-(dibenzofuran-2-yloxy)aniline, which was used directly for further transformation without further purification.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07737285B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-5f9ed205d452444faefb95035ce5c199
출처 메모uspto-grants-2010_06