Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1'-Carbonyldiimidazole → hexahydroimidazo[1,5-a]pyridin-3(2H)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| 반응물 | Piperidine-2-methylamine | HCID 90865 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | hexahydroimidazo[1,5-a]pyridin-3(2H)-one | HCID 47002315 | — |
반응 단계
A solution of CDI (830 mg, 5.1 mmol) and piperidin-2-ylmethanamine (520 mg, 4.6 mmol) in DCM (20 mL) was stirred at room temperature overnight. After the solvent was removed, the residue was directly used for the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09260452B2 |
| 출처 데이터셋 | uspto-grants-2016_02 |
| ORD ID | ord-619ee6518b044e9c8f2128490bba4c10 |
| 출처 메모 | uspto-grants-2016_02 |