2-Amino-5-cyanopyridine → Phenyl (5-cyanopyridin-2-yl)carbamate

HRID 1778019노트

반응식

HRID 1778019 반응식
NC1C=CC(C#N)=CN=1.[C:10]1([O:16][C:17](=[O:32])[NH:18][C:19]2[CH:24]=[C:23](OCCOC)[C:22]([C:30]#[N:31])=[CH:21][N:20]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:10]1([O:16][C:17](=[O:32])[NH:18][C:19]2[CH:24]=[CH:23][C:22]([C:30]#[N:31])=[CH:21][N:20]=2)[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

참가 물질

3

반응물 2

HCID 8182602-Amino-5-cyanopyridineHCID 125470569Phenyl (5-cyano-4-(2-methoxyethoxy)pyridin-2-yl)carbamate

생성물 1

HCID 57469773Phenyl (5-cyanopyridin-2-yl)carbamate

실험 절차

From 2-amino-5-cyanopyridine, reacted in an analogous manner to the preparation of intermediate 108. (UPLC-MS 6) tR 0.92; ESI-MS 240.1 [M+H]+.

출처 및 근거

ORD 기록
ord-7c1bceba99d94614a9c13100d9243a4d
출처 데이터셋
uspto-grants-2016_02
특허 번호
US09266883B2

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