2-(Dimethoxymethyl)-1,8-naphthyridine → 2-(Dimethoxymethyl)-7-methyl-1,8-naphthyridine

HRID 1778026노트

반응식

HRID 1778026 반응식
[NH2:1][C:2]1[N:9]=[C:8]([CH3:10])[CH:7]=[CH:6][C:3]=1[CH:4]=O.[CH3:11][O:12][CH:13]([O:24][CH3:25])[C:14]1[CH:23]=CC2C(=NC=CC=2)N=1>>[CH3:11][O:12][CH:13]([O:24][CH3:25])[C:14]1[CH:23]=[CH:4][C:3]2[C:2](=[N:9][C:8]([CH3:10])=[CH:7][CH:6]=2)[N:1]=1

참가 물질

3

반응물 2

HCID 177501752-(Dimethoxymethyl)-1,8-naphthyridineHCID 534010302-Amino-6-methylnicotinaldehyde

생성물 1

HCID 1180367962-(Dimethoxymethyl)-7-methyl-1,8-naphthyridine

실험 절차

From 2-amino-6-methylnicotinaldehyde, synthesized in an analogous manner to intermediate 5, the title compound was obtained as a white solid. (UPLC-MS 6) tR 0.62; ESI-MS 219.2 [M+H]+.

출처 및 근거

ORD 기록
ord-dc54c846cfff49169468ecad758908c6
출처 데이터셋
uspto-grants-2016_02
특허 번호
US09266883B2

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