참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tert-Butylamine | HCID 6385 | — |
| 반응물 | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-tert-butyl-3-chloropropane-1-sulfonamide | HCID 11701296 | 99% |
반응 단계
tert-Butylamine (3.0 mol, 315.3 mL) was dissolved in THF (2.5 L). The solution was cooled to −20° C. 3-Chloropropanesulfonyl chloride (1.5 mol, 182.4 mL) was added slowly. The reaction mixture was allowed to warm to rt and stirred for 24 h. The mixture was filtered, and the filtrate was concentrated in vacuo. The residue was dissolved in CH2Cl2 (2.0 L). The resulting solution was washed with 1 N HCl (1.0 L), water (1.0 L), brine (1.0 L) and dried over Na2SO4. It was filtered and concentrated in vacuo to give a slightly yellow solid, which was crystallized from hexane to afford the product as a white solid (316.0 g, 99%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07741281B2 |
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| 출처 데이터셋 | uspto-grants-2010_06 |
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| ORD ID | ord-4d152abc044543a395564c614ea0d57a |
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| 출처 메모 | uspto-grants-2010_06 |
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