Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propyl isocyanate → 1-Propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propyl isocyanate | HCID 61033 | — |
| 반응물 | 1-Methoxymethylcyclopropylsulfonylamine tert-butylcarbamate | HCID 66752382 | — |
| 생성물 | 1-Propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate | HCID 66753294 | 100% |
반응 단계
This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate except that 1.10 equivalents of n-propyl isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.10 (m, 2H), 0.51 (m, 2H), 0.67 (m, 1H), 1.10 (m, 2H), 1.49 (s, 9H), 1.62 (m, 2H), 1.87 (d, J=7.0 Hz, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741281B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-d02dce065cef470d8f389fc3a6d68a94 |
| 출처 메모 | uspto-grants-2010_06 |