Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobenzene → 4-Benzeneazodiphenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobenzene | HCID 2272 | — |
| 용매 | Aniline | HCID 6115 | — |
| 생성물 | 4-Benzeneazodiphenylamine | HCID 7575 | 90% |
반응 단계
A solution of 25% aqueous tetramethylammonium hydroxide (8 mL) was concentrated under vacuum at 75° C. until solid material formed. Azobenzene (1.8 g) and aniline (10 mL) were added and the solution was stirred under the same conditions for 4 hours and then in the presence of air for 12 hours. Analysis of the reaction by HPLC revealed 90% yield of 4-(phenylazo)diphenylamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05633407 |
| 출처 데이터셋 | uspto-grants-1997_05 |
| ORD ID | ord-f24cc0230cab430e999525bce7ab4a89 |
| 출처 메모 | uspto-grants-1997_05 |