2-Aminophenol → HCID 23106862, 화합물

HRID 1782552

반응식

HRID 1782552 반응식
I[CH:2]([CH2:4][CH2:5][CH2:6][CH3:7])[CH3:3].[NH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[OH:15]>>[CH3:3][CH:2]([NH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[OH:15])[CH2:4][CH2:5][CH2:6][CH3:7]

참가 물질

3

반응물 2

HCID 58012-AminophenolHCID 330192-Iodohexane

생성물 1

HCID 23106862HCID 23106862, 화합물

실험 절차

The same procedure as in Example 4 was repeated except for using 2-iodohexane in place of 2-iodobutane, to conduct the reaction. As a result, it was confirmed that the rate of conversion of o-aminophenol was 93%, the selectivity to the N-monoalkylated compound was 41% and the oxygen absorption initiation time as an index of determining an oxidation-inhibiting property thereof was 320 min.

후처리

  1. customthe reaction
  2. customthe oxygen absorption initiation time as an index

출처 및 근거

ORD 기록
ord-a4f48cb693294aaea3c29805e7a8377b
출처 데이터셋
uspto-grants-2009_03
특허 번호
US07498467B2

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