Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Aminophenol → HCID 23106862, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Aminophenol | HCID 5801 | — |
| 반응물 | 2-Iodohexane | HCID 33019 | — |
| 생성물 | HCID 23106862 | HCID 23106862 | — |
반응 단계
The same procedure as in Example 6 was repeated except that the molar ratio of 2-iodohexane to o-aminophenol was changed to 0.8, the 2-iodohexane was dropped over 4.5 h, and then the reaction mixture was stirred at room temperature for 0.5 h. As a result, it was confirmed that the rate of conversion of o-aminophenol was 71%, the selectivity to the N-monoalkylated compound was 86%, and the oxygen absorption initiation time as an index of determining an oxidation-inhibiting property thereof was 320 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07498467B2 |
| 출처 데이터셋 | uspto-grants-2009_03 |
| ORD ID | ord-25de0d922c614920bc11e2d755fc570c |
| 출처 메모 | uspto-grants-2009_03 |