참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethylorthoformate | HCID 53630039 | — |
| 반응물 | 2-Cyclopropylamino-5-nitrobenzenesulphonamide | HCID 67530158 | — |
| 생성물 | 4-cyclopropyl-7-nitro-4H-1,2,4-benzothiadiazine 1,1-dioxide | HCID 67530771 | — |
반응 단계
In a round-bottom flask, a mixture of 2-cyclopropylamino-5-nitrobenzenesulphonamide (5 g), originating from the Step above, and ethyl orthoformate (50 mL) is heated in the open state at 130° C. for 3 hours. The suspension obtained is cooled on an ice bath and the insoluble material is collected by filtration, washed with ether and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07741320B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-d3c399511b97447abf51faf290d79fe9 |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
