4-(Dimethylamino)phenylboronic acid → 4-(4'-Dimethylamino-biphenyl-4-yloxymethyl)-5-methyl-furan-2-carboxylic acid
반응식
I[C:2]1[CH:18]=[CH:17][C:5]([O:6][CH2:7][C:8]2[CH:9]=[C:10]([C:14]([OH:16])=[O:15])[O:11][C:12]=2[CH3:13])=[CH:4][CH:3]=1.[CH3:19][N:20]([CH3:30])[C:21]1[CH:26]=[CH:25][C:24](B(O)O)=[CH:23][CH:22]=1>>[CH3:19][N:20]([CH3:30])[C:21]1[CH:26]=[CH:25][C:24]([C:2]2[CH:18]=[CH:17][C:5]([O:6][CH2:7][C:8]3[CH:9]=[C:10]([C:14]([OH:16])=[O:15])[O:11][C:12]=3[CH3:13])=[CH:4][CH:3]=2)=[CH:23][CH:22]=1참가 물질
3
실험 절차
Compound (113) was prepared from compound (26) and (4-dimethylamino-phenyl)-boronic acid by adapting the procedure of Example 27B. LC/MS System B; Rt=1.83 mins, m/z (ES−)=350 (M−H for C21H21NO4).
출처 및 근거
- ORD 기록
- ord-c93c2c2b2c82485bbc72c0e49d1a1560
- 출처 데이터셋
- uspto-grants-2009_03
- 특허 번호
- US07507754B2
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