n-Propylimidazole → HCID 178456359, 화합물

HRID 1789471노트

반응식

HRID 1789471 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11]Cl)=[CH:4][CH:3]=1.[CH2:13]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH2:14][CH3:15]>>[Cl-:1].[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][CH2:11][N+:18]2[CH:19]=[CH:20][N:16]([CH2:13][CH2:14][CH3:15])[CH:17]=2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 118785n-PropylimidazoleHCID 200827321-Chloro-4-(4-chlorobutyl)benzene

생성물 1

HCID 178456359HCID 178456359, 화합물

반응 조건

온도
130 °C

실험 절차

Add 7.13 g (0.035 mole) of 1-chloro-4-(4-chlorobutyl)benzene to 3.52 g (0.032 mole) of 1-propyl-1H-imidazole and heat to 130° C. for 18 hours. Follow the progress of reaction by NMR (CDCl3). At the completion of the reaction, cool to room temperature to obtain the title compound.

후처리

  1. customthe progress of reaction by NMR (CDCl3)
  2. customAt the completion of the reaction
  3. temperaturecool to room temperature

출처 및 근거

ORD 기록
ord-560edb78e0de42889fc1ab50fda17b06
출처 데이터셋
uspto-grants-1987_08
특허 번호
US04689341

반응 노트

불러오는 중…