Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4-methylpyridine → N-(4-Methyl-2-pyridyl)acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4-methylpyridine | HCID 1533 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | N-(4-Methyl-2-pyridyl)acetamide | HCID 220485 | 95% |
반응 단계
2-Amino4-methylpyridine (99.0 g, 91.5 mmol) in acetic anhydride (250 mL) was warmed to 70° C. for two h. The mixture was cooled to room temperature and diethyl ether (100 mL) added. The product crystallized as white needle crystals. Filtering and drying in vacuo afforded N-(4-methyl-pyridin-2-yl)-acetamide (130 g, 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07071175B1 |
| 출처 데이터셋 | uspto-grants-2006_07 |
| ORD ID | ord-4c91d3469d9e4eeeb3d52c80632ed8db |
| 출처 메모 | uspto-grants-2006_07 |