2,4-Dichlorobenzylidenemalononitrile → HCID 10194700, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([NH2:15])=[NH:14])[CH:7]=[CH:6]2.[Cl:16][C:17]1[CH:28]=[C:27]([Cl:29])[CH:26]=[CH:25][C:18]=1[CH:19]=[C:20]([C:23]#[N:24])[C:21]#[N:22]>>[NH2:24][CH2:23][C:20]1[C:21]([NH2:22])=[N:14][C:13]([C:8]2[CH:7]=[CH:6][C:5]3[C:10](=[CH:11][CH:12]=[C:3]([O:2][CH3:1])[CH:4]=3)[CH:9]=2)=[N:15][C:19]=1[C:18]1[CH:25]=[CH:26][C:27]([Cl:29])=[CH:28][C:17]=1[Cl:16]

참가 물질

반응물 2

HCID 180892,4-Dichlorobenzylidenemalononitrile

HCID 32749176-Methoxy-naphthalene-2-carboxamidine

생성물 1

HCID 10194700HCID 10194700, 화합물

실험 절차

The title compound, MS: m/e=425.0 (M+H+), was prepared from 6-methoxy-naphthalene-2-carboxamidine and 2-(2,4-dichloro-benzylidene)-malononitrile in analogy to the process described in Example 11 as a solid.

출처 및 근거

ORD 기록: ord-5bf31a4a82c54a659a4b5f03f532a80f
출처 데이터셋: uspto-grants-2006_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07022718B2

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