Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glutarimide → 1-[2-(2-Bromophenyl)ethyl]piperidine-2,6-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glutarimide | HCID 70726 | — |
| 반응물 | 2-(2-Bromophenyl)ethan-1-ol | HCID 2734089 | — |
| 반응물 | 3-[2-(2-Bromophenyl)ethyl]-1-methylimidazolidine-2,4-dione | HCID 9857394 | — |
| 생성물 | 1-[2-(2-Bromophenyl)ethyl]piperidine-2,6-dione | HCID 9965964 | — |
반응 단계
2-Bromophenethyl alcohol (402 mg, 2 mmol) and glutarimide (317 mg, 2.8 mmol) were treated as described in the preparation of compound 436. Purification was done by flash chromatography (petroleum ether/ethyl acetate 2:1) to provide the title compound as a colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07034015B2 |
| 출처 데이터셋 | uspto-grants-2006_04 |
| ORD ID | ord-6775be51e7b949f590d83bb994f20fc5 |
| 출처 메모 | uspto-grants-2006_04 |