4-Nitrobenzaldehyde → HCID 178498134, 화합물
반응식
[NH2:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][CH:3]=1.[N+:12]([C:15]1[CH:22]=[CH:21][C:18]([CH:19]=O)=[CH:17][CH:16]=1)([O-:14])=[O:13]>C(O)C>[N+:12]([C:15]1[CH:22]=[CH:21][C:18](/[CH:19]=[N:1]/[C:2]2[CH:3]=[CH:4][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:10][CH:11]=2)=[CH:17][CH:16]=1)([O-:14])=[O:13]참가 물질
4
실험 절차
A mixture of methyl 4-aminobenzoate (1.51 g, 10 mmol) and 4-nitrobenzaldehyde (1.51 g, 10 mmol) in ethanol (30 mL) was stirred overnight to give the yellow slurry. The precipitated off-white solid was collected and dried in vacuo to give (E)-methyl 4-(4-nitrobenzylideneamino)benzoate (2.93 g, 95% yield).
후처리
- customto give the yellow slurry
- customThe precipitated off-white solid was collected
- customdried in vacuo
출처 및 근거
- ORD 기록
- ord-1ae6f3957d4647b9b2551f960ebad5ea
- 출처 데이터셋
- uspto-grants-2013_01
- 특허 번호
- US08344137B2
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