참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 4-Butoxy-3-methoxybenzonitrile | HCID 4458757 | — |
| 생성물 | 2-Nitro-4-n-butoxy-5-methoxybenzonitrile | HCID 58367817 | — |
반응 단계
3-methoxy-4-n-butoxybenzonitrile (1.282 g, 6 mmol) and nitric acid (6 mL) were added into a round bottom flask, heated to 30° C. to react for 2 h, poured into ice-water; after complete stirring, the solution was filtered, washed with water and air-dried to yield 1.495 g of light yellow solid product with a recovery rate of 96%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08349835B2 |
|---|
| 출처 데이터셋 | uspto-grants-2013_01 |
|---|
| ORD ID | ord-4be8465a9a8e4f788b126a6aa277adbf |
|---|
| 출처 메모 | uspto-grants-2013_01 |
|---|
