Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → 3-(Propan-2-yl)benzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Water | HCID 962 | — |
| 반응물 | 1-Bromo-3-isopropylbenzene | HCID 138499 | — |
| 반응물 | HCID 178418260 | HCID 178418260 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 3-(Propan-2-yl)benzonitrile | HCID 258440 | — |
반응 단계
5.15 g (25.87 mmol) m-bromo-isopropyl-benzene and 2.69 g (30.04 mmol) copper cyanide are stirred in 2.50 ml of pyridine for 24 hours at 180° C. Then 15 ml of water, 15 ml of toluene and 15 ml conc. ammonia solution are added, then the mixture is extracted. The organic phase is dried and evaporated to dryness.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08354418B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-656f53ae722d463c8e6a0eff14f36527 |
| 출처 메모 | uspto-grants-2013_01 |