Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylate → 4-(1H-Pyrazol-1-yl)piperidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-butyl 4-(1H-pyrazol-1-yl)piperidine-1-carboxylate | HCID 67971778 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4-(1H-Pyrazol-1-yl)piperidine | HCID 21193045 | 96% |
반응 단계
The title compound from Step B above (50 mg, 0.2 mmol) was dissolved in 4 M HCl in dioxane (2.0 mL) and stirred at RT for 1 h. The product was concentrated under reduced pressure and dried under high vacuum to give the title compound (i-17) (30 mg, 96%). ESI-MS calculated for C81H13N3: Exact Mass: 151.11. Found 152.10.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08354403B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-82c09d36b50e44e199295577f8c352ee |
| 출처 메모 | uspto-grants-2013_01 |