Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | L-Tyrosine | HCID 6057 | — |
| 반응물 | L-Phenylalanine | HCID 6140 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | propan-2-yl (2S)-2-amino-3-phenylpropanoate hydrochloride | HCID 15599949 | — |
| 생성물 | propan-2-yl (2S)-2-amino-3-(4-hydroxyphenyl)propanoate hydrochloride | HCID 67262861 | — |
반응 단계
Excess HCl gas was added with stirring to a suspension of L-phenylalanine or L-tyrosine in excess isopropanol. The mixture was heated to reflux for 16 h, and then the volatiles were evaporated under vacuum to give L-phenylalanine isopropyl ester hydrochloride or L-tyrosine isopropyl ester hydrochloride of sufficient purity for immediate use.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741328B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-733fefb0a17c4d6aa12ad2ef65fce39e |
| 출처 메모 | uspto-grants-2010_06 |