Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-Chloro-1-(chloromethyl)-2-methoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4 Chloro-2-methoxybenzyl alcohol | HCID 3549393 | — |
| 생성물 | 4-Chloro-1-(chloromethyl)-2-methoxybenzene | HCID 18523560 | 95% |
반응 단계
Step A In a manner similar to the method described in Example 57 Step A, 4-chloro-2-methoxybenzyl alcohol (Aldrich) (4.9 g, 28 mmol) was reacted with thionyl chloride (20 mL) to give 4-chloro-2-methoxybenzyl chloride as a white solid (5.1 g, 95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08354444B2 |
| 출처 데이터셋 | uspto-grants-2013_01 |
| ORD ID | ord-df22fcf813f049ad88970e596e1a4c2e |
| 출처 메모 | uspto-grants-2013_01 |