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Glycine tert-butyl ester → HCID 178443624, 화합물

HRID 1806852
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HRID 1806852 반응식
[C:1]([O:5][C:6](=[O:9])[CH2:7][NH2:8])([CH3:4])([CH3:3])[CH3:2].[CH3:10][C:11]([CH3:18])([CH:15]([CH3:17])[CH3:16])[CH2:12][CH:13]=O>C(Cl)Cl>[C:1]([O:5][C:6](=[O:9])[CH2:7]/[N:8]=[CH:13]/[CH2:12][C:11]([CH3:18])([CH3:10])[CH:15]([CH3:17])[CH3:16])([CH3:4])([CH3:3])[CH3:2]
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참가 물질

4

반응물 2

HCID 151417Glycine tert-butyl esterHCID 124253353,3,4-Trimethylpentanal

생성물 1

HCID 178443624HCID 178443624, 화합물수율 80.7%

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Step D In a manner similar to the method described in Example 1a, glycine tert-butyl ester (1 g, 7.7 mmol) was reacted with 3,3,4-trimethyl-pentanal (1.1 g, 8 mmol) in CH2Cl2 at room temperature for 5 h to give [3,3,4-trimethyl-pent-(E)-ylideneamino]-acetic acid tert-butyl ester as a colorless oil (1.5 g, 80%).

출처 및 근거

ORD 기록
ord-110f75357df64c9490e40fd8f9ab3abb
출처 데이터셋
uspto-grants-2013_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08354444B2

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