1,1'-Carbonyldiimidazole → HCID 86649530, 화합물
반응식
[C:1]([C:5]1[S:6][C:7]2[CH2:17][CH2:16][C:11]3[N:12]=[C:13]([NH2:15])[S:14][C:10]=3[C:8]=2[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[CH:18]1[N:22]=[CH:21][N:20]([C:23](N2C=NC=C2)=[O:24])[CH:19]=1>C(Cl)Cl>[C:1]([C:5]1[S:6][C:7]2[CH2:17][CH2:16][C:11]3[N:12]=[C:13]([NH:15][C:23]([N:20]4[CH:19]=[CH:18][N:22]=[CH:21]4)=[O:24])[S:14][C:10]=3[C:8]=2[N:9]=1)([CH3:4])([CH3:2])[CH3:3]참가 물질
4
실험 절차
7-tert-Butyl-4,5-dihydro-benzo[1,2-d;3,4-d′]bisthiazol-2-ylamine (Stage T.1, 175 mg, 0.659 mmol) was dissolved in DCM (10 mL), CDI (297 mg, 1.648 mmol) was then added, and the RM was stirred at rt for 2 h. The title compound was isolated by filtration, washed with DCM and dried under HV.
출처 및 근거
- ORD 기록
- ord-a89f3efb50a844c9b4891e2888af7d4a
- 출처 데이터셋
- uspto-grants-2013_01