돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1809202생성일: 2026년 10월 26일

Trifluoroacetic acid → HCID 86655088, 화합물

https://huagongshe.com/reaction/1809202

반응식

참여 물질

역할이름HCID투입량
반응물Trifluoroacetic acidHCID 6422—
반응물3-Cyanobenzene-1-sulfonamideHCID 2808718—
촉매PalladiumHCID 23938—
용매EthanolHCID 702—
생성물HCID 86655088HCID 86655088—

반응 단계

TFA (5 mL) can be added to a solution of 3-cyano-benzenesulfonamide (0.90 g, 4.94 mmol) in EtOH (50 mL) followed by Pd/C (100 mg) and the mixture hydrogenated at 40 psi and r.t. for 20 h. The reaction mixture can be filtered through celite and the solvent concentrated to give 3-Aminomethyl-benzenesulfonamide TFA salt as a white solid in quantitative yield.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08362018B2
출처 데이터셋uspto-grants-2013_01
ORD IDord-e4e9a0a35d394ab39795a9e29dcf9336
출처 메모uspto-grants-2013_01