2-Bromo-4-methylbenzaldehyde → (2'-Formyl-6-methoxy-5'-methyl-biphenyl-3-yl)-acetic acid ethyl ester

HRID 1810496

반응식

HRID 1810496 반응식
[CH2:1]([O:3][C:4](=[O:23])[CH2:5][C:6]1[CH:11]=[CH:10][C:9]([O:12][CH3:13])=[C:8](B2OC(C)(C)C(C)(C)O2)[CH:7]=1)[CH3:2].Br[C:25]1[CH:32]=[C:31]([CH3:33])[CH:30]=[CH:29][C:26]=1[CH:27]=[O:28]>>[CH2:1]([O:3][C:4](=[O:23])[CH2:5][C:6]1[CH:7]=[C:8]([C:25]2[CH:32]=[C:31]([CH3:33])[CH:30]=[CH:29][C:26]=2[CH:27]=[O:28])[C:9]([O:12][CH3:13])=[CH:10][CH:11]=1)[CH3:2]

참가 물질

3

반응물 2

HCID 46452922-Bromo-4-methylbenzaldehydeHCID 58120060[4-Methoxy-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acetic acid ethyl ester

생성물 1

HCID 58148809(2'-Formyl-6-methoxy-5'-methyl-biphenyl-3-yl)-acetic acid ethyl ester

실험 절차

Prepared according to the procedure described in Example 1, Step 4, using the following starting materials: [4-methoxy-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-acetic acid ethyl ester and 2-bromo-4-methylbenzaldehyde.

후처리

  1. customPrepared

출처 및 근거

ORD 기록
ord-f0582750b55b4d91a0013adb7e237cb2
출처 데이터셋
uspto-grants-2013_01
특허 번호
US08362044B2

연결된 노트

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