2-(2-Chlorobenzenesulfonyl) acetonitrile → 2-(2-Chlorobenzene-1-sulfonyl)-3,3-di(methanesulfonyl)prop-2-enenitrile

반응식

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([CH2:11][C:12]#[N:13])(=[O:10])=[O:9].ClC1C=C[C:18]([S:21]([CH2:24]C#N)(=[O:23])=[O:22])=CC=1>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8]([C:11](=[C:24]([S:8]([CH3:3])(=[O:10])=[O:9])[S:21]([CH3:18])(=[O:23])=[O:22])[C:12]#[N:13])(=[O:10])=[O:9]

참가 물질

반응물 2

HCID 7182462-(2-Chlorobenzenesulfonyl) acetonitrile

HCID 7358292-(4-Chlorobenzenesulfonyl)acetonitrile

생성물 1

HCID 225044652-(2-Chlorobenzene-1-sulfonyl)-3,3-di(methanesulfonyl)prop-2-enenitrile

실험 절차

The titled compound was prepared in an analogous fashion to Intermediate 2 except that 2-(2-chlorobenzenesulfonyl) acetonitrile is utilized in place of 2-(4-chlorobenzenesulfonyl) acetonitrile.

출처 및 근거

ORD 기록: ord-fcb8dd93ac3346b6b6701f8b8fc6a3c5
출처 데이터셋: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06875771B2

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