Hydroxylamine → 2,4-Dimethoxybenzaldoxime

HRID 1814396

반응식

[CH3:1][O:2][C:3]1[CH:11]=[C:10]([O:12][CH3:13])[CH:9]=[CH:8][C:4]=1[C:5](O)=O.[NH2:14][OH:15]>>[CH3:1][O:2][C:3]1[CH:11]=[C:10]([O:12][CH3:13])[CH:9]=[CH:8][C:4]=1[CH:5]=[N:14][OH:15]

참가 물질

반응물 2

HCID 787Hydroxylamine

HCID 70522,4-Dimethoxybenzoic acid

생성물 1

HCID 2312422,4-Dimethoxybenzaldoxime

실험 절차

2,4-Dimethoxybenzoic acid is reacted with hydroxylamine to form 2,4-dimethoxybenzaldoxime. 2,4-Dimethoxybenzaldoxime is reacted with diphosphorus pentoxide to form 2,4-dimethoxybenzonitrile. 2,4-Dimethoxybenzonitrile is reacted with boron trichloride to form 2,4-dihydroxybenzonitrile.

출처 및 근거

ORD 기록: ord-503264449ebb4d298bd88087feb785e8
출처 데이터셋: uspto-grants-2005_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06875883B2

연결된 노트

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