N-methyl-2-toluamide → HCID 22503279, 화합물

HRID 1814515노트

반응식

HRID 1814515 반응식
[CH3:1][NH:2][C:3](=[O:11])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH3:10].[CH3:12][O:13][CH2:14][CH2:15][CH2:16][C:17]1[CH:24]=[CH:23][C:20](C#N)=[CH:19][CH:18]=1>>[CH3:12][O:13][CH2:14][CH2:15][CH2:16][C:17]1[CH:24]=[CH:23][C:20]([C:1]2[NH:2][C:3](=[O:11])[C:4]3[C:5]([CH:10]=2)=[CH:6][CH:7]=[CH:8][CH:9]=3)=[CH:19][CH:18]=1

참가 물질

3

반응물 2

HCID 75111N-methyl-2-toluamideHCID 225033794-(3-Methoxypropyl)benzonitrile

생성물 1

HCID 22503279HCID 22503279, 화합물수율 26.9%

실험 절차

According to the method of Example 10-1, N-methyl-2-methylbenzamide (3.75 g) and 4-(3-methoxypropyl)benzonitrile (4.40 g) were reacted, to give 3-[4-(3-methoxypropyl)phenyl]isoquinolin-1-one (1.98 g).

후처리

  1. customwere reacted

출처 및 근거

ORD 기록
ord-a18b2c8a2eaa4ffb9bf2f57ce171e860
출처 데이터셋
uspto-grants-2005_04
특허 번호
US06875761B2

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