Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Camphor-10-sulfonyl chloride → N-{4-[4-amino-2-(ethoxymethyl)-6-methyl-1H-imidazo[4,5-c]pyridin-1-yl]butyl}1-[(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Camphor-10-sulfonyl chloride | HCID 88856 | — |
| 반응물 | 1-(4-aminobutyl)-2-ethoxymethyl-6-methyl-1H-imidazo[4,5-c]pyridin-4-amine | HCID 12972960 | — |
| 생성물 | N-{4-[4-amino-2-(ethoxymethyl)-6-methyl-1H-imidazo[4,5-c]pyridin-1-yl]butyl}1-[(1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulfonamide | HCID 60067120 | — |
반응 단계
Using the method of Examples 32-46, D-(+)-10-camphorsulfonyl chloride was reacted with 1-(4-aminobutyl)-2-ethoxymethyl-6-methyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired product. The observed accurate mass was 565.2720.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06878719B2 |
| 출처 데이터셋 | uspto-grants-2005_04 |
| ORD ID | ord-c9079a9fab714c7085dcbb7796167779 |
| 출처 메모 | uspto-grants-2005_04 |