Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methylamine → Melamine, methyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | 1,3,5-Triazine-2,4-diamine, 6-chloro- | HCID 18831 | — |
| 생성물 | Melamine, methyl- | HCID 26029 | 65% |
반응 단계
A mixed solution comprising 14.5 g (0.1 mol) of 2,4-diamino-6-chloro-1,3,5-triazine synthesized in Reference Example 1 and 31.1 g (0.4 mol) of 40% aqueous solution of methylamine was heated under stirring and reacted finally at the reflux temperature thereof for 6 hours. After cooling the reacted solution, products were filtered off, and washed with cold water. The resulting filter residue was dried in vacuo at 70° C. for 6 hours to give 9.1 g (yield: 65%) of the titled compound. Malting point: 269° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06878824B2 |
| 출처 데이터셋 | uspto-grants-2005_04 |
| ORD ID | ord-db82ff322d4b4ffa9331772067bb510c |
| 출처 메모 | uspto-grants-2005_04 |